There is therefore still a need to develop experimental methodologies to obtain or derive accurate sistem parameters.
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The adiabatic isolation of the stationary phase would probably be a huge step forward in UHPLC and supercritical fluid chromatography (SFC) and the idea and design suggested by Fabrice Gritti–called a vacuum jacketed column–is obviously marvelous. Through this the detrimental band broadening caused by frictional thermal effects could be eliminated and I would expect the commercialization of such columns to be seen in the near future.
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In other loyalbahis work you have carried out fundamental studies in which the effect of longitudinal temperature gradient on retention, caused by frictional heating, was experimentally dissociated from the combined effect of pressure and frictional heating (3).
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